Please prepare your samples in the designated area or under a hood, and not on top of the magnet. The chemical shifts (d) of solvent signals observed for 1 H NMR and 13 C NMR spectra are listed in the ...
For the majority of users conducting nuclear magnetic resonance (NMR) spectroscopy today, sample preparation follows a similar path: isolate a compound or compounds from a reaction mixture (or if ...
What synthetic chemist hasn't wistfully lingered over a reaction flask, longing for a simple, informative way of following the chemistry without exposing sensitive reagents to air and moisture? A ...
There are federal training requirements about the dangers of the NMR magnets and the danger of helium asphyxiation that need to be taught to anybody entering the NMR room PS13. Unauthorized persons ...
Have your data emailed to you when the acquisition is completed! Use this instrument for 1H, 19F, 19F{1H}, 13C, 11B, 31P, 29Si, 195Pt, or practically any "X" nucleus with automatic probe-tuning. This ...
Despite urinary biomarkers being successfully used to diagnose and monitor a range of central nervous system disorders, including demyelinating, neurodegenerative, and motor neuron diseases, ...
NMR spectra are typically collected in solutions made up of deuterated solvents due to the fact that a protonated solvent will yield large solvent peaks which may hide the solute’s spectral features.